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Microwave-mediated synthesis of N-methyliminodiacetic acid (MIDA) boronates
journal contribution
posted on 2023-06-08, 20:40 authored by Adam J Close, Paul Kemmitt, Matthew K Emmerson, John SpencerJohn SpencerA library of over 20, mainly aryl or heteroaryl, N-methyliminodiacetic acid (MIDA) boronates have been synthesised. A rapid microwave-mediated (MW) method (5–10 min) has been developed using polyethylene glycol 300 (PEG 300) as solvent. However, acetonitrile (MeCN) and dimethylformamide (DMF) were found to be alternative solvents, the latter especially for 2-substituted aryl boronic acids.
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Publication status
- Published
File Version
- Accepted version
Journal
TetrahedronISSN
0040-4020Publisher
ElsevierExternal DOI
Issue
47Volume
70Page range
9125-9131Department affiliated with
- Chemistry Publications
Full text available
- Yes
Peer reviewed?
- Yes
Legacy Posted Date
2015-05-01First Open Access (FOA) Date
2015-05-01First Compliant Deposit (FCD) Date
2015-05-01Usage metrics
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