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Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state
journal contribution
posted on 2023-06-08, 18:34 authored by Christine B Baltus, Neil J Press, Milan D Antonijevic, Graham J Tizzard, Simon J Coles, John SpencerJohn SpencerA biphenyl library incorporating amide and sulfonamide groups has been synthesised via microwave -mediated Suzukie-Miyaura couplings. Many derivatives were crystallised from dichloromethane/methanol and analysed by single crystal X-ray diffraction. An interesting structure was obtained for N-(40-methylbiphenyl-4-yl)acetamide with Z0¼6 and hydrogen-bonding networks of the type NeH.O in the unit cell.
History
Publication status
- Published
Journal
TetrahedronISSN
0040-4020Publisher
ElsevierExternal DOI
Issue
45Volume
68Page range
9272-9277Department affiliated with
- Chemistry Publications
Full text available
- No
Peer reviewed?
- Yes
Legacy Posted Date
2014-09-30Usage metrics
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