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171Yb cross-polarization magic angle spinning NMR spectroscopic studies of organometallic compounds:? bis(cyclopentadienyl) derivatives

journal contribution
posted on 2023-06-07, 23:02 authored by Julian M Keates, Gerard A Lawless
A series of nine Yb(II) bis(cyclopentadienyl) complexes have been studied by 171Yb CP MAS (cross polarization magic angle spinning) NMR spectroscopy. The optimization of the cross polarization conditions are described. The proton T1? values have been determined. The spinning side band manifold for each compound has been analyzed. The derived chemical shift tensor data are discussed with respect to molecular structure elucidation.

History

Publication status

  • Published

Journal

Organometallics

Publisher

American Chemical Society

Issue

13

Volume

16

Page range

2842 - 2846

ISBN

0276-7333

Department affiliated with

  • Chemistry Publications

Full text available

  • No

Peer reviewed?

  • Yes

Legacy Posted Date

2012-02-06

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