Microwave-mediated synthesis of N-methyliminodiacetic acid (MIDA) boronates

Close, Adam J, Kemmitt, Paul, Emmerson, Matthew K and Spencer, John (2014) Microwave-mediated synthesis of N-methyliminodiacetic acid (MIDA) boronates. Tetrahedron, 70 (47). pp. 9125-9131. ISSN 0040-4020

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Abstract

A library of over 20, mainly aryl or heteroaryl, N-methyliminodiacetic acid (MIDA) boronates have been synthesised. A rapid microwave-mediated (MW) method (5–10 min) has been developed using polyethylene glycol 300 (PEG 300) as solvent. However, acetonitrile (MeCN) and dimethylformamide (DMF) were found to be alternative solvents, the latter especially for 2-substituted aryl boronic acids.

Item Type: Article
Schools and Departments: School of Life Sciences > Chemistry
Subjects: Q Science > QD Chemistry
Depositing User: John Spencer
Date Deposited: 01 May 2015 07:19
Last Modified: 06 Mar 2017 07:51
URI: http://sro.sussex.ac.uk/id/eprint/53847

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